Übersetzung für "Suction temperature" in Deutsch

The yellow precipitate was filtered off with suction at room temperature and washed with ether.

The crystalline product is filtered with suction at room temperature and dried.

Then it was cooled to room temperature, suction filtered and washed with cold ethanol.

The precipitated condensation product is filtered off with suction at room temperature and dried.

The precipitate formed is stirred for 16 hours at ambient temperature, suction filtered and dried.

The precipitate was filtered off with suction at room temperature and recrystallized from toluene.

The solids are filtered off with suction at room temperature and dried.

The reaction product was filtered off with suction at room temperature, washed with water until chloride-free and dried.

The resulting crystal suspension is stirred for 1 hour at room temperature, suction-filtered, and washed neutral with water.

The aqueous product suspension is filtered under suction at room temperature and the yellow crystalline product is washed with water until it is free of chloride.

The mixture is stirred overnight at ambient temperature, suction filtered to remove the molecular sieve and the solvent is evaporated off.

The precipitate which separates out is filtered off under suction at room temperature, washed with n-butanol and recrystallized from ethanol.

The evaporation residue is extracted by boiling with 200 ml of acetone, and the resulting suspension is filtered with suction at room temperature.

The toluene was removed in a rotary evaporator, and the solid which remained was filtered off with suction at room temperature and washed a number of times with MeOH.

The reaction mixture is heated at reflux for 3 hours and the solid is filtered off with suction at room temperature and dried.

The crystals are filtered with suction at room temperature, washed with CH2 Cl2 and dried.

The residue was stirred for 1 hour in 400 ml of acetonitrile at room temperature, suction filtered, and dried.

The precipitated hemiester was filtered off with suction at room temperature, washed 3 times with toluene and dried at 50° in vacuo.

This is filtered off with suction at room temperature, repeatedly washed with water and dried at 100° C. in vacuo.

However, solely temperature-based control has proven to be insufficient, since the temperature of the oil is also affected by suction pressure, the temperature of the environment and the temperature of the pumped medium.

After the reaction had ended (check by TLC), the excess acylating agent was destroyed with water and the resulting precipitate was filtered off with suction at room temperature.

After the absorption of hydrogen had ceased, the catalyst was filtered off hot and the resulting precipitate was filtered off with suction at room temperature.

The mixture was stirred for a further 4 h at room temperature and 1 h at 50° C., and subsequently filtered by suction at room temperature.

The white precipitate is filtered off with suction at room temperature, washed with toluene and then with water, and dried.

For further purification, the moist crude product is boiled up with 100 ml of water, filtered off with suction at room temperature, washed with H2 O and dried to constant weight over CaCl2 at 100° C. in a vacuum drying cabinet.